The Owens College Course of Practical Organic ChemistryMacmillan, 1887 - 200 páginas |
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Página x
... Potassium benzene sulphonate 22 23 26 • 28 29 31 • 33 35 37 39 99 XIV . Anisol XV . • 4I Ortho- and para - nitrophenol • 42 XVI . " " Picric acid • 45 XVII . 92 Phenolphthalein 46 " " XVIII . Quinone . . 48 " " XIX . Hydroquinone 50 24 ...
... Potassium benzene sulphonate 22 23 26 • 28 29 31 • 33 35 37 39 99 XIV . Anisol XV . • 4I Ortho- and para - nitrophenol • 42 XVI . " " Picric acid • 45 XVII . 92 Phenolphthalein 46 " " XVIII . Quinone . . 48 " " XIX . Hydroquinone 50 24 ...
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... Potassium ethyl sulphate . 106 • 36 XLVIII . Propionitril 107 33 XLIX . Propionic acid . 109 L. Ethylene dibromide IIO LI . Ethylene alcohol • 113 13 LII . Ethylene chlorhydrin 114 LIII . 29 Succinic acid . • 117 LIV . Dibromsuccinic ...
... Potassium ethyl sulphate . 106 • 36 XLVIII . Propionitril 107 33 XLIX . Propionic acid . 109 L. Ethylene dibromide IIO LI . Ethylene alcohol • 113 13 LII . Ethylene chlorhydrin 114 LIII . 29 Succinic acid . • 117 LIV . Dibromsuccinic ...
Página 34
... potassium carbonate or caustic soda solution added in the cold . The yellow colour of the salt changes to green and the free base , which is formed , is extracted with ether . On evaporating off the ether the base remains in the form of ...
... potassium carbonate or caustic soda solution added in the cold . The yellow colour of the salt changes to green and the free base , which is formed , is extracted with ether . On evaporating off the ether the base remains in the form of ...
Página 36
... On evaporating down the hydrochloric acid solution on the water - bath colourless crystals of dimethylamine hydrochloride may be obtained . PREPARATION XII . POTASSIUM BENZENE SULPHONATE , CH , .SOK 36 PRACTICAL ORGANIC CHEMISTRY .
... On evaporating down the hydrochloric acid solution on the water - bath colourless crystals of dimethylamine hydrochloride may be obtained . PREPARATION XII . POTASSIUM BENZENE SULPHONATE , CH , .SOK 36 PRACTICAL ORGANIC CHEMISTRY .
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Julius Berend Cohen. PREPARATION XII . POTASSIUM BENZENE SULPHONATE , CH , .SOK . LITERATURE . - Mitscherlich ( 1834 ) , Pogg . Ann . 31 , 283 and 364 ; Michael , Adair ( 1877 ) , Ber . 10 , 585 . 100 grms ... Potassium benzene sulphonate 22.
Julius Berend Cohen. PREPARATION XII . POTASSIUM BENZENE SULPHONATE , CH , .SOK . LITERATURE . - Mitscherlich ( 1834 ) , Pogg . Ann . 31 , 283 and 364 ; Michael , Adair ( 1877 ) , Ber . 10 , 585 . 100 grms ... Potassium benzene sulphonate 22.
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50 grms absolute alcohol acetic acid action aldehyde allyl ammonia ammonium anhydrous aniline aromatic Assistant-Master atom benzaldehyde benzene benzoic acid benzoyl chloride benzyl boiling calcium chloride Cambridge caustic potash caustic soda chloroform cold colour colourless compound conc containing cooling Crown 8vo crystals decomposes dilute dissolved distilled ELEMENTARY ethylene bromide evolution Extra fcap fatty Fcap Fellow of Trinity Fifty grms filtered filtrate Fittig formed fumes Globe 8vo glycerin Greek grms H₂O heated hot water hundred grms hydrochloric acid hydrogen iodide John's College late Fellow layer litre capacity LL.D mesitylene mixture nitric acid oxalic acid Pharm phenol phosphorus Phys potassium carbonate potassium cyanide powdered Prep PREPARATION PRIMER Professor Properties.-Colourless liquid purified reaction reflux condenser residue retort revised round-bottomed flask salt School separated slowly added small quantity soda solution sodium solidifies soluble in water sulphuric acid temperature Trinity College tube vessel washed water-bath
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