Manual of Chemical Analysis as Applied to the Examination of Medicinal Chemicals: A Guide for the Determination of Their Identity and Quality and for the Detection of Impurities and Adulterations : for the Use of Pharmaceutists, Physicians, Druggists, and Manufacturing Chemists, and of Pharmaceutical and Medical Students

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D. Appleton, 1877 - 393 páginas
 

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Página 327 - of hydrochloric acid, and allow it to macerate for 24 hours. Transfer the whole to a small percolator, and, after the fluid has ceased to drop, add at intervals about an ounce and a half of similarly acidulated water, or until the fluid which passes through is free from
Página 66 - quantity of air is now sucked out of flask B by means of the tube d, whereby the air in A is likewise rarefied. On allowing the air to return, a quantity of the sulphuric acid ascends to the tube c, and flows over into flask A, causing a disengagement of
Página 1 - CHEMICAL ANALYSIS AS APPLIED TO THE EXAMINATION OF MEDICINAL CHEMICALS. A GUIDE FOR THE DETERMINATION OF THEIR IDENTITY AND QUALITY, AND
Página 327 - ceased to drop, add at intervals about an ounce and a half of similarly acidulated water, or until the fluid which passes through is free from color. Add to the percolated fluid, solution of
Página 327 - until nearly the whole of the coloring-matter has been removed, taking care that the fluid remains acid in reaction. Filter, and wash with
Página 327 - grains of potassium hydrate, or as much as will cause the precipitate, which is at first formed, to be nearly redissolved, and
Página 365 - for about two minutes. If the spirit is free from methylic alcohol, the solution darkens, and often assumes transiently a purplish tinge, but continues quite
Página 363 - there until it has acquired that temperature, will boil distinctly on the addition of a few small pieces of glass.
Página 389 - Pb Li Mg Mn Hg Mo Ni N O P Pt K Se Si Ag Na Sr S Sn Zn
Página 157 - Argentic nitrate is soluble in an equal weight of cold, and in half that quantity of boiling, water ; it is also

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